![]() ![]() Cryogenic electron microscopy further reveals intimate contact between LNMO and LiPON without noticeable structure and chemical composition evolution after extended cycling, demonstrating the superior stability of LiPON against a high voltage cathode. Neutron depth profiling indicates a slight overlithiated layer at the interface prior to cycling, a result that is consistent with the excess charge capacity measured during the first cycle. ![]() With Li metal as the anode, this system can deliver stable performance for 600 cycles with an average Coulombic efficiency >99%. In this work, a thin-film battery consisting of an LNMO cathode with a solid lithium phosphorus oxynitride (LiPON) electrolyte is tested and their interface before and after cycling is characterized. In contrast, some solid-state electrolytes have a wide electrochemical stability range and can withstand the required oxidative potential. However, in liquid electrolyte cells, the high voltage causes continuous cell degradation through the oxidative decomposition of carbonate-based liquid electrolytes. Spinel-type LiNi 0.5Mn 1.5O 4 (LNMO) is one of the most promising 5 V-class cathode materials for Li-ion batteries that can achieve high energy density and low production costs.
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